Preparation of 2,6-di-tert-butyl-4-mercaptophenol_Kain Industrial Additive
Background and overview[1] 2,6-di-tert-butyl-4-mercaptophenol can be used as a pharmaceutical synthesis intermediate and can be used in laboratory research and development and chemical and pharmaceutical synthesis processes. Preparation[1] Step 1: 2,6-di-tert-butyl-4-thiocyanatophenol Add 2,6-di-tert-butylphenol (2.06g, 10mmol), NaBr (1.02g, 10mmol), and NaSCN (1.62g, 20mmol) to a three-necked flask containing MeOH (30mL), respectively. The mixture was cooled in…